Observation of two-stage crystallization of poly(ether ether ketone) by thermal mechanical analysis

Hsin Lung Chen; Roger S. Porter

doi:10.1016/0032-3861(93)90169-B

Observation of two-stage crystallization of poly(ether ether ketone) by thermal mechanical analysis

Hsin Lung Chen, Roger S. Porter^*

^*Corresponding author for this work

University of Massachusetts

Research output: Contribution to journal › Journal Article › peer-review

6 Scopus citations

Abstract

We report the application of thermal mechanical analysis (t.m.a.) to studying the crystallization behaviour of poly(ether ether ketone) (PEEK). We are able to show that the two crystallization stages of PEEK are clearly distinguished by measuring the variation of film thickness with time during isothermal crystallization. These two crystallization stages cannot be readily distinguished by d.s.c. The distinction by t.m.a. becomes less clear with increasing crystallization temperature due to overlap of the two crystallization stages.

Original language	English
Pages (from-to)	4576-4578
Number of pages	3
Journal	Polymer
Volume	34
Issue number	21
DOIs	https://doi.org/10.1016/0032-3861(93)90169-B
State	Published - 11 1993
Externally published	Yes

Keywords

poly(ether ether ketone)
primary crystallization
secondary crystallization
two-stage crystallization

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10.1016/0032-3861(93)90169-B

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title = "Observation of two-stage crystallization of poly(ether ether ketone) by thermal mechanical analysis",

abstract = "We report the application of thermal mechanical analysis (t.m.a.) to studying the crystallization behaviour of poly(ether ether ketone) (PEEK). We are able to show that the two crystallization stages of PEEK are clearly distinguished by measuring the variation of film thickness with time during isothermal crystallization. These two crystallization stages cannot be readily distinguished by d.s.c. The distinction by t.m.a. becomes less clear with increasing crystallization temperature due to overlap of the two crystallization stages.",

keywords = "poly(ether ether ketone), primary crystallization, secondary crystallization, two-stage crystallization",

author = "Chen, {Hsin Lung} and Porter, {Roger S.}",

year = "1993",

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doi = "10.1016/0032-3861(93)90169-B",

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volume = "34",

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journal = "Polymer",

issn = "0032-3861",

publisher = "Elsevier B.V.",

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TY - JOUR

T1 - Observation of two-stage crystallization of poly(ether ether ketone) by thermal mechanical analysis

AU - Chen, Hsin Lung

AU - Porter, Roger S.

PY - 1993/11

Y1 - 1993/11

N2 - We report the application of thermal mechanical analysis (t.m.a.) to studying the crystallization behaviour of poly(ether ether ketone) (PEEK). We are able to show that the two crystallization stages of PEEK are clearly distinguished by measuring the variation of film thickness with time during isothermal crystallization. These two crystallization stages cannot be readily distinguished by d.s.c. The distinction by t.m.a. becomes less clear with increasing crystallization temperature due to overlap of the two crystallization stages.

AB - We report the application of thermal mechanical analysis (t.m.a.) to studying the crystallization behaviour of poly(ether ether ketone) (PEEK). We are able to show that the two crystallization stages of PEEK are clearly distinguished by measuring the variation of film thickness with time during isothermal crystallization. These two crystallization stages cannot be readily distinguished by d.s.c. The distinction by t.m.a. becomes less clear with increasing crystallization temperature due to overlap of the two crystallization stages.

KW - poly(ether ether ketone)

KW - primary crystallization

KW - secondary crystallization

KW - two-stage crystallization

UR - http://www.scopus.com/inward/record.url?scp=0027698384&partnerID=8YFLogxK

U2 - 10.1016/0032-3861(93)90169-B

DO - 10.1016/0032-3861(93)90169-B

M3 - 文章

AN - SCOPUS:0027698384

SN - 0032-3861

VL - 34

SP - 4576

EP - 4578

JO - Polymer

JF - Polymer

IS - 21

ER -

Observation of two-stage crystallization of poly(ether ether ketone) by thermal mechanical analysis

Abstract

Keywords

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